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Synthesis and characterization of nateglinide derivatives by Sharma Rajdeep
Synthesis and characterization of nateglinide derivatives by Sharma Rajdeep
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Synthesis and characterization of nateglinide derivatives

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Description

A series of seven nateglinide analogues were synthesized successfully using 4-isopropyl cyclohexyl carboxylic acid (trans acid) as starting material, react with thionyl chloride and formed trans-4-isopropyl cyclohexane carbonyl chloride (trans acid chloride) as an intermediate which further reacted with D-phenylalanine to yield nateglinide. The derivatives were synthesized by reacting nateglinide and ethylchloroformate, and formed an unstable mix anhydride compound, which further react with primary and secondary amines to yield the nateglinide derivatives. All these molecules were characterized spectroscopically by mass spectra, IR, 1H NMR.
Release date Australia
August 8th, 2015
Audience
  • General (US: Trade)
Pages
96
Dimensions
152x229x6
ISBN-13
9783659769207
Product ID
24003824

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